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Handbook of Inductively Coupled Plasma Mass Spectrometry

Jarvis K.E.
Heftet / 2012 / Engelsk

Produktdetaljer

ISBN
9789401053556
Publisert
2012-10-26
Utgiver
Vendor
Springer
Høyde
229 mm
Bredde
152 mm
Aldersnivå
Research, P, 06
Språk
Product language
Engelsk
Format
Product format
Heftet

Forfatter
Jarvis K.E.

Handbook of Inductively Coupled Plasma Mass Spectrometry

Jarvis K.E.
Heftet / 2012 / Engelsk
Jarvis K.E.
Heftet / 2012 / Engelsk
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Since the introduction of the first commercial inductively coupled plasma mass spectrometry (ICP-MS) instruments in 1983, the technique has gained rapid and wide acceptance in many analytical laboratories. There are now well over 400 instruments installed worldwide, which are being used in a range of disciplines for the analysis of geological, environmental, water, medical, biological, metallurgical, nuclear and industrial samples. Experience oflCP-MS in many laboratories is limited, and there is therefore a need for a handbook containing practical advice in addition to fundamental informa­ tion. Such a handbook would be useful not only to users new to the technique, but also to users with some experience who wish to expand their knowledge of the subject. Therefore we have written this book for users in a variety of fields with differing levels of experience and expertise. The first two chapters provide a brief history of ICP-MS and discussions of design concepts, ICP physical processes, and fundamental principles of instrument operation. Armed with this background knowledge, users will be better equipped to evaluate advantages and limitations of the technique. Detailed descriptions and information for instrumental components are provided in chapter 3. Subsequent chapters deal with the practical aspects of sample analysis by ICP-MS. Whether samples are to be analysed in liquid, solid ·or gaseous form is always an important consideration, and there is a wide choice of sample introduction techniques.
Les mer
Since the introduction of the first commercial inductively coupled plasma mass spectrometry (ICP-MS) instruments in 1983, the technique has gained rapid and wide acceptance in many analytical laboratories.
Les mer
1 Origins and development.- 1.1. Introduction.- 1.2 The ICP-MS system.- 2 Instrumentation for ICP-MS.- 2.1 The inductively coupled plasma.- 2.2 Ion extraction.- 2.3 Ion focusing.- 2.4 Quadrupole mass spectrometers.- 2.5 Other mass spectrometers.- 2.6 Ion detection.- 2.7 Vacuum considerations.- 3 Instrument options.- 3.1 Introduction.- 3.2 Nebulisers.- 3.3 Spray chambers.- 3.4 Torches.- 3.5 Interface.- 4 Sample introduction for liquids and gases.- 4.1 Introduction.- 4.2 Electrothermal vaporisation.- 4.3 Vapour generation and gas phase sample introduction.- 4.4 Liquid chromatography.- 4.5 Flow injection.- 4.6 Direct sample insertion.- 5 Interferences.- 5.1 Introduction.- 5.2 Spectroscopic interferences.- 5.3 Non-spectroscopic interferences.- 6 Calibration and data handling.- 6.1 Introduction.- 6.2 General concepts.- 6.3 Instrumental modes of data collection.- 6.4 Linearity of response.- 6.5 Blanks.- 6.6 Factors affecting signal stability.- 6.7 Qualitative analysis.- 6.8 Semi-quantitative calibration.- 6.9 Quantitative analysis.- 7 Sample preparation for ICP-MS.- 7.1 Introduction.- 7.2 General considerations.- 7.3 Digestion procedures.- 7.4 Separation and pre-concentration methods.- 7.5 Conclusions and overview.- 8 Elemental analysis of solutions and applications.- 8.1 Introduction.- 8.2 Multi-element determinations.- 8.3 Geological applications.- 8.4 Environmental applications.- 8.5 Nuclear applications.- 8.6 Industrial applications.- 8.7 Biological applications.- 8.8 Summary.- 9 The analysis of natural waters by ICP-MS.- 9.1 Introduction.- 9.2 Water sampling procedures for ICP-MS.- 9.3 Direct water analysis by ICP-MS.- 9.4 Water analysis with chemical separation and/or pre-concentration.- 9.5 Calibration strategies.- 10 Analysis of solid samples.- 10.1 Introduction.- 10.2 Slurry nebulisation.- 10.3 Laser ablation.- 10.4 Direct sample insertion.- 10.5 Powdered solids.- 10.6 Arc nebulisation.- 11 Isotope ratio measurement.- 11.1 Introduction.- 11.2 Instrument performance.- 11.3 Applications and methods of isotope analysis.- Appendices.- Appendix 1 Originators of reference material cited in the text.- Appendix 2 Naturally-occurring isotopes—useful data.- Appendix 3 Glossary.- References.
Les mer
Springer Book Archives
Springer Book Archives
GPSR Compliance The European Union's (EU) General Product Safety Regulation (GPSR) is a set of rules that requires consumer products to be safe and our obligations to ensure this. If you have any concerns about our products you can contact us on ProductSafety@springernature.com. In case Publisher is established outside the EU, the EU authorized representative is: Springer Nature Customer Service Center GmbH Europaplatz 3 69115 Heidelberg, Germany ProductSafety@springernature.com
Les mer

Relaterte produkter

Since the introduction of the first commercial inductively coupled plasma mass spectrometry (ICP-MS) instruments in 1983, the technique has gained rapid and wide acceptance in many analytical laboratories. There are now well over 400 instruments installed worldwide, which are being used in a range of disciplines for the analysis of geological, environmental, water, medical, biological, metallurgical, nuclear and industrial samples. Experience oflCP-MS in many laboratories is limited, and there is therefore a need for a handbook containing practical advice in addition to fundamental informa­ tion. Such a handbook would be useful not only to users new to the technique, but also to users with some experience who wish to expand their knowledge of the subject. Therefore we have written this book for users in a variety of fields with differing levels of experience and expertise. The first two chapters provide a brief history of ICP-MS and discussions of design concepts, ICP physical processes, and fundamental principles of instrument operation. Armed with this background knowledge, users will be better equipped to evaluate advantages and limitations of the technique. Detailed descriptions and information for instrumental components are provided in chapter 3. Subsequent chapters deal with the practical aspects of sample analysis by ICP-MS. Whether samples are to be analysed in liquid, solid ·or gaseous form is always an important consideration, and there is a wide choice of sample introduction techniques.
Les mer
Since the introduction of the first commercial inductively coupled plasma mass spectrometry (ICP-MS) instruments in 1983, the technique has gained rapid and wide acceptance in many analytical laboratories.
Les mer
1 Origins and development.- 1.1. Introduction.- 1.2 The ICP-MS system.- 2 Instrumentation for ICP-MS.- 2.1 The inductively coupled plasma.- 2.2 Ion extraction.- 2.3 Ion focusing.- 2.4 Quadrupole mass spectrometers.- 2.5 Other mass spectrometers.- 2.6 Ion detection.- 2.7 Vacuum considerations.- 3 Instrument options.- 3.1 Introduction.- 3.2 Nebulisers.- 3.3 Spray chambers.- 3.4 Torches.- 3.5 Interface.- 4 Sample introduction for liquids and gases.- 4.1 Introduction.- 4.2 Electrothermal vaporisation.- 4.3 Vapour generation and gas phase sample introduction.- 4.4 Liquid chromatography.- 4.5 Flow injection.- 4.6 Direct sample insertion.- 5 Interferences.- 5.1 Introduction.- 5.2 Spectroscopic interferences.- 5.3 Non-spectroscopic interferences.- 6 Calibration and data handling.- 6.1 Introduction.- 6.2 General concepts.- 6.3 Instrumental modes of data collection.- 6.4 Linearity of response.- 6.5 Blanks.- 6.6 Factors affecting signal stability.- 6.7 Qualitative analysis.- 6.8 Semi-quantitative calibration.- 6.9 Quantitative analysis.- 7 Sample preparation for ICP-MS.- 7.1 Introduction.- 7.2 General considerations.- 7.3 Digestion procedures.- 7.4 Separation and pre-concentration methods.- 7.5 Conclusions and overview.- 8 Elemental analysis of solutions and applications.- 8.1 Introduction.- 8.2 Multi-element determinations.- 8.3 Geological applications.- 8.4 Environmental applications.- 8.5 Nuclear applications.- 8.6 Industrial applications.- 8.7 Biological applications.- 8.8 Summary.- 9 The analysis of natural waters by ICP-MS.- 9.1 Introduction.- 9.2 Water sampling procedures for ICP-MS.- 9.3 Direct water analysis by ICP-MS.- 9.4 Water analysis with chemical separation and/or pre-concentration.- 9.5 Calibration strategies.- 10 Analysis of solid samples.- 10.1 Introduction.- 10.2 Slurry nebulisation.- 10.3 Laser ablation.- 10.4 Direct sample insertion.- 10.5 Powdered solids.- 10.6 Arc nebulisation.- 11 Isotope ratio measurement.- 11.1 Introduction.- 11.2 Instrument performance.- 11.3 Applications and methods of isotope analysis.- Appendices.- Appendix 1 Originators of reference material cited in the text.- Appendix 2 Naturally-occurring isotopes—useful data.- Appendix 3 Glossary.- References.
Les mer
Springer Book Archives
Springer Book Archives
GPSR Compliance The European Union's (EU) General Product Safety Regulation (GPSR) is a set of rules that requires consumer products to be safe and our obligations to ensure this. If you have any concerns about our products you can contact us on ProductSafety@springernature.com. In case Publisher is established outside the EU, the EU authorized representative is: Springer Nature Customer Service Center GmbH Europaplatz 3 69115 Heidelberg, Germany ProductSafety@springernature.com
Les mer

Produktdetaljer

ISBN
9789401053556
Publisert
2012-10-26
Utgiver
Vendor
Springer
Høyde
229 mm
Bredde
152 mm
Aldersnivå
Research, P, 06
Språk
Product language
Engelsk
Format
Product format
Heftet

Forfatter
Jarvis K.E.

Relaterte produkter